Chemical assembly of the heteronuclear pivalate complex with the LiI and FeIII ions View Full Text


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Article Info

DATE

2018-03

AUTHORS

I. А. Lutsenko, М. А. Kiskin, G. G. Alexandrov, V. K. Imshennik, Yu. V. Maksimov, A. V. Khoroshilov, A. S. Goloveshkin, А. А. Sidorov, I. L. Eremenko

ABSTRACT

The heteronuclear complex [Fe4Li2(O)2(Piv)10(H2O)2] (1, Piv is the pivalic acid anion) was obtained by refluxing FeIII pivalates with LiI pivalates in toluene and isolated as the 1•PhCH3 solvate with a toluene molecule. According to X-ray diffraction data, complex 1 contains the {Fe4Li2O2} core. The Mössbauer spectroscopy data indicate that the core comprises para magnetic FeIII ions in the high-spin state located in the symmetric octahedral environment of oxygen atoms. Thermolysis of 1 studied by simultaneous thermal analysis demonstrated thermal stability of the complex up to 225 °С. The main end product of thermolysis at 600 °С is the mixed oxide LiFe5O8. More... »

PAGES

449-454

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URI

http://scigraph.springernature.com/pub.10.1007/s11172-018-2091-x

DOI

http://dx.doi.org/10.1007/s11172-018-2091-x

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https://app.dimensions.ai/details/publication/pub.1105106450


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N-Triples is a line-based linked data format ideal for batch operations.

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Turtle is a human-readable linked data format.

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RDF/XML is a standard XML format for linked data.

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This table displays all metadata directly associated to this object as RDF triples.

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