Paramagnetic CuII complexes with 1-(hetarylmethyl)silatranes View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-12

AUTHORS

T. I. Vakul’skaya, S. S. Khutsishvili, D. V. Pavlov, Yu. I. Bolgova, I. V. Sterkhova, O. M. Trofimova

ABSTRACT

The structures of paramagnetic complexes CuCl2•L with L = HetCH2Si(OCH2CH2)3N [Het = pyrrol-1-yl (1), indol-1-yl (2), carbazol-9-yl (3), imidazole-1-yl (4), 3,5-dimethylpyrazol-1-yl (5), 1,2,4-triazol-1-yl (6), benzimidazol-1-yl (7), and 1,2,3-benzotriazol-1-yl (8)] were studied by the ESR and quantum chemical methods in terms of the density functional theory (DFT) approximation. The difference in structures of complexes CuCl2•1—CuCl2•8 is mainly determined by the nature of the five-membered heterocycle. The ESR spectra at room temperature are typical of the mononuclear complexes of CuII of axial symmetry with various types of distortions. In complexes CuCl2•1—CuCl2•3, narrow symmetric signals of zero-valent copper are recorded. These signals remain in the spectra for at least six months, which can characterize them as efficient stabilizing matrices of nanoparticles. More... »

PAGES

2276-2282

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-017-2014-2

DOI

http://dx.doi.org/10.1007/s11172-017-2014-2

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1101548409


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