Synthesis and structure of 4,6-di(tert-butyl)-2-(4-chloro-7,8-dimethylquinolin-2-yl)-7-(piperidin-1-ylmethyl)-1,3-tropolone View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-11

AUTHORS

V. V. Tkachev, Yu. A. Sayapin, I. V. Dorogan, A. A. Kolodina, E. A. Gusakov, V. N. Komissarov, G. V. Shilov, S. M. Aldoshin, V. I. Minkin

ABSTRACT

The reaction of 4-chloro-2,7,8-trimethylquinoline with 4,6-di(tert-butyl)-3-(piperidin- 1-ylmethyl)-1,2-benzoquinone, which was prepared by the in situ oxidation of 4,6-di(tert- butyl)-3-(piperidin-1-ylmethyl)pyrocatechol with sodium nitrite, gave 4,6-di(tert-butyl)-2- (4-chloro-7,8-dimethylquinolin-2-yl)-7-(piperidin-1-ylmethyl)-1,3-tropolone. Its structure was determined by X-ray diffraction. The energy and structural characteristics of the tauto- mers of this compound in the gas phase and in a polar solution were calculated by quantum chemical methods (PBE0/6-311+G(d,p)). More... »

PAGES

2136-2141

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-017-1993-3

DOI

http://dx.doi.org/10.1007/s11172-017-1993-3

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1101535661


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155 schema:name Institute of Problems of Chemical Physics, Russian Academy of Sciences, 1 prosp. Akad. Semenova, 142432, Chernogolovka, Moscow Region, Russian Federation
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157 grid-institutes:grid.465325.3 schema:alternateName Southern Scientific Center, Russian Academy of Sciences, 41 ul. Chekhova, 344006, Rostov-on-Don, Russian Federation
158 schema:name Institute of Physical and Organic Chemistry, Southern Federal University, 194/2 prosp. Stachki, 344090, Rostov-on-Don, Russian Federation
159 Southern Scientific Center, Russian Academy of Sciences, 41 ul. Chekhova, 344006, Rostov-on-Don, Russian Federation
160 rdf:type schema:Organization
 




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