Ferrocenecarboxylic acid and microwave-assisted synthesis of ferrocenoyl hydrazones View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-03

AUTHORS

V. N. Kulikov, R. S. Nikulin, D. E. Arkhipov, A. N. Rodionov, E. S. Babusenko, L. V. Kovalenko, Yu. A. Belousov

ABSTRACT

A protocol to access ferrocenecarboxylic acid via carboxylation of ferrocene with carbon dioxide in the presence of aluminum chloride was elaborated. An efficient microwave-assisted synthesis of ferrocenoyl hydrazones by condensation of ferrocene carbohydrazide with carbonyl compounds was developed. Structures of the synthesized compounds were examined by NMR spectroscopy and mass spectrometry. Structures of N´-(4-chlorobenzylidene)ferrocenecarbohydrazide, N´-(4-methoxybenzylidene)ferrocenecarbohydrazide, and N´-(2-hydroxybenzylidene)ferrocenecarbohydrazide were determined by X-ray diffraction analysis. Synthesized compounds were found to have no toxicity against P. aeruginosa, E. coli, S. aureus, B. subtilis, M. rubrum, and C. albicans. More... »

PAGES

537-544

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-017-1768-x

DOI

http://dx.doi.org/10.1007/s11172-017-1768-x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1091406181


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