Synthesis and structure of new 3,7-diazabicyclo[3.3.1]nonane derivatives View Full Text


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Article Info

DATE

2016-09

AUTHORS

E. A. Chigorina, K. A. Frolov, V. V. Dotsenko, A. S. Goloveshkin, I. S. Bushmarinov, S. G. Krivokolysko

ABSTRACT

Aminomethylation of triethylammonium 4-aryl-3,5-dicyano-6-oxo-1,4,5,6-tetrahydropyridin-2-olates and their sulfur and selenium analogs, as well as the structure of formed products, were studied in details. The reaction is of general character and leads to the formation of 7-substituted 9-aryl-2,4-dioxo-, 9-aryl-4-oxo-2-thioxo-, 9-aryl-4-oxo-2-selenoxo-3,7-diazabicyclo[3.3.1]nonane derivatives or their salts. The structures of ethyl 9-(2-chlorophenyl)-5-cyano-7-(4-methylphenyl)-2-oxo-4-thioxo-3,7-diazabicyclo[3.3.1]nonane-1-carboxylate (as a complex with N-methylmorpholine) and triethylammonium salt of 7-benzyl-4-oxo-2-selenoxo-9-(2-thienyl)-3,7-diazabicyclo[3.3.1]nonane-1,5-dicarbonitrile were studied by X-ray crystallography. More... »

PAGES

2260-2269

References to SciGraph publications

  • 2011-10. New approach to the synthesis of 4-aryl-3,5-dicyano-6-oxo- 1,4,5,6-tetrahydropyridin-2-olates (salts of guareschi imides) in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 2015-02. Synthesis of partially hydrogenated 1,3,5-thiadiazines by Mannich reaction in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 2016-02. Aminomethylation of morpholinium and N-methylmorpholinium 3,5-dicyano-4,4-dimethyl-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolates in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 2007-12. The Mannich reaction in the synthesis of N,S-containing heterocycles 8. Aminomethylation of 3,5-dicyano-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolates as a method for the synthesis of new functionally substituted 3,7-diazabicyclo[3.3.1]nonane derivatives in RUSSIAN CHEMICAL BULLETIN
  • 2012-06. Synthesis and properties of triethylammonium 4-aryl(hetaryl)-3,5-dicyano-6-oxo-1,4,5,6-tetrahydro-pyridine-2-selenolates in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 2000-03. N-Methylmorpholinium 4-aryl-5-cyano-3-methoxycarbonyl-2-oxo-1,2,3,4-tetrahydropyridine-6-thiolates: synthesis and properties in RUSSIAN CHEMICAL BULLETIN
  • 2013-07. 1-(Cyanoacetyl)-3,5-dimethylpyrazole as an effective alternative to cyanoacetic ester in the synthesis of 2,6-dioxopiperidine-3,5-dicarbonitrile derivatives in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 2005-11. Aminomethylation of 1,2,3,4-Tetrahydropyridine-6-thiolates: A Novel Approach to Synthesis of 3,7-Diazabicyclo[3.3.1]nonane Derivatives in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 2013-02. The First Example of 3,7-Diazabicyclo[3.3.1]nonane Synthesis by Aminomethylation of Guareschi Imide Salts in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 2005-08. Synthesis, crystal structures, and electrochemistry of CuII complexes with tetradentate N2O2 ligands derived from 3,7-diazabicyclo[3.3.1]nonan-9-one in RUSSIAN CHEMICAL BULLETIN
  • 2007-05. A Double Mannich-type Reaction in the 1,4,5,6-Tetrahydropyridine-2-thiolate Series: A Convenient Approach to Functionalized 3,7-Diazabicyclo[3.3.1]nonane Derivatives in MONATSHEFTE FÜR CHEMIE - CHEMICAL MONTHLY
  • 2012-05. Application of a Nickel-Bispidine Complex as Pre-Catalyst for C(sp2)–C(sp3) Bond Formations in CATALYSIS LETTERS
  • 2013-08. Chemistry of cyanoselenoacetamide (Review) in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
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