An unusual reduction route of 2,4,6-trinitrobenzoic acid under conditions of aqueous-phase hydrogenation over Pd/Sibunit catalyst View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2016-06

AUTHORS

R. M. Mironenko, O. B. Belskaya, V. P. Talzi, V. A. Rodionov, S. V. Sysolyatin, V. A. Likholobov

ABSTRACT

For the first time it was established that the catalytic hydrogenation of 2,4,6-trinitrobenzoic acid to 1,3,5-triaminobenzene can proceed via the formation of aromatic hydroxyamines and cyclohexane-1,3,5-trione trioxime. As a result of aqueous-phase hydrogenation of sodium salt of 2,4,6-trinitrobenzoic acid in the presence of 5%Pd/Sibunit catalyst at a temperature of 323 K and pressure of 0.5 MPa, a trioxime in high yield (about 70 %) was obtained. Due to high selectivity to cyclohexane-1,3,5-trione trioxime the catalytic hydrogenation of sodium salt of 2,4,6-trinitrobenzoic acid can be considered as a new method for its synthesis. More... »

PAGES

1535-1540

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-016-1479-8

DOI

http://dx.doi.org/10.1007/s11172-016-1479-8

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1083899084


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