Bimetallic 3d—4f-molecules [MEu(ButCOO)5(1,10-phen)] (M = Zn2+, Co2+, phen is phenanthroline): synthesis, structure, luminescent and magnetic properties View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2016-06

AUTHORS

M. A. Kiskin, Zh. V. Dobrokhotova, A. S. Bogomyakov, S. A. Kozyukhin, V. Yu. Timoshenko, I. L. Eremenko

ABSTRACT

New heterometallic complexes [MEu(Piv)5(1,10-phen)]•MeCN (M = Zn2+ (1), Co2+ (2), Piv– = ButCOO–, 1,10-phen is 1,10-phenanthroline) were obtained. Luminescence spectra of compound 1 reveal a metal-centered Eu3+ luminescence, the luminescence lifetime is about 1 ms. Using TGA and DSC methods, it was shown that [ZnEu(Piv)5(1,10-phen)] is a stable binuclear molecule undergoing a structural transformation in the 210—230 °C temperature range, which leads to a partial transition of the sample into the glass state. Complex 2 does not exhibit luminescence due to the presence of high-spin cobalt(II) ions. The magnetic behavior of 2 according to calculations based on the molecular field model is determined by spin-orbit interactions of cobalt(II) and europium(III) ions. More... »

PAGES

1488-1494

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-016-1475-z

DOI

http://dx.doi.org/10.1007/s11172-016-1475-z

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1083907121


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