A novel water-soluble sulfide cluster of iron: synthesis, properties, and intercalation into molybdenum disulfide View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-01

AUTHORS

A. V. Anyushin, E. V. Korotaev, A. Yu. Andreeva, M. R. Ryzhikov, D. A. Mainichev, M. N. Sokolov, V. P. Fedin

ABSTRACT

A novel water-soluble sulfide cluster of iron, {Fe6S8[P(CH2OH)3]6}2+, was obtained from ferrous chloride tetrahydrate, tris(hydroxymethyl)phosphine, and H2S in methanol. A reaction of the cluster in solution with dispersed molybdenum disulfide gave an inclusion compound, MoS2({Fe6S8[P(CH2OH)3]6}Cl2)0.06. The products obtained were characterized by IR, NMR, and ESR spectroscopy, electronic absorption spectroscopy, mass spectrometry, and elemental analysis. The magnetic susceptibility of the cluster was studied in solution and in a molybdenum disulfide matrix. More... »

PAGES

173-180

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-016-1280-8

DOI

http://dx.doi.org/10.1007/s11172-016-1280-8

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1051396928


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275 schema:name A. V. Nikolaev Institute of Inorganic Chemistry, Siberian Branch of the Russian Academy of Sciences, 3 prosp. Akad. Lavrent’eva, 630090, Novosibirsk, Russian Federation
276 Novosibirsk State University, 2 ul. Pirogova, 630090, Novosibirsk, Russian Federation
277 rdf:type schema:Organization
 




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