New 8-aryl-8´-iodo derivatives of cobalt bis(1,2-dicarbollide) View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2015-03

AUTHORS

I. D. Kosenko, I. A. Lobanova, I. V. Ananyev, Z. A. Starikova, J. N. Laskova, V. I. Bregadze

ABSTRACT

Reactions of 8,8´-μ-iodo-3-commo-3-cobalta[bis(1,2-dicarba-closo-dodecaborane)] (8,8´-μI-3,3´-Co(1,2-C2B9H10)2) with aryl halides (fluoro-, chloro-, bromo-, iodo-, and o-dichlorobenzenes) were studied. The reaction of 8,8´-μ-I-3,3´-Co(1,2-C2B9H10)2 with these reagents proceeded only in the presence of sterically hindered Lewis bases with the cleavage of the bridging B—I bond and the formation of the corresponding anionic 8-aryl-8´-iodo derivatives of cobalt bis(1,2-dicarbollide). X-ray diffraction studies were carried out for the charge-compensated 8´-iodo-8-(4,1-oxathian-1-ium)icosahydro-1,1´,2,2´-tetracarba-3-commo-cobaltacloso-tricosaborate and the anionic tetramethylpiperidinium 8´-(3,4-dichlorophenyl)-8-iodoicosahydro-1,1´,2,2´-tetracarba-3-commo-cobalta-closo-tricosaborate. The X-ray diffraction data showed that the molecule of the former compound has the gauche conformation, whereas the anionic complex is in the trans conformation. More... »

PAGES

704-711

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-015-0923-5

DOI

http://dx.doi.org/10.1007/s11172-015-0923-5

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1018884603


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