Structural studies of conformers of 3-(N-acetyl-N-arylamino)tropones by heteronuclear, two-dimensional, and dynamic NMR spectroscopy and X-ray diffraction analysis View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2015-03

AUTHORS

I. G. Borodkina, A. A. Kolodina, P. B. Chepurnoi, Yu. A. Sayapin, E. A. Gusakov, I. V. Dorogan, G. S. Borodkin, G. V. Shilov, V. V. Tkachev

ABSTRACT

Acylation of 5,7-di(tert-butyl)-2-(5,8-dimethyl-4-piperidinoquinolin-2-yl)-3-(3,5-dimethylphenylamino)tropone leads to the corresponding 3-(N-acetyl-N-arylamino)tropone. Heteronuclear, two-dimensional, and dynamic NMR spectroscopy were used to determine structures of conformers of N-acetyl-3-arylaminotropone. The structure of 3-[N-acetyl-N(3,5-dimethylphenyl)amino]-5,7-di(tert-butyl)-2-(5,8-dimethyl-4-piperidinoquinolin-2-yl)tropone was established by X-ray diffraction studies.

PAGES

650-657

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-015-0913-7

DOI

http://dx.doi.org/10.1007/s11172-015-0913-7

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1016826222


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