36-Nuclear CoII and NiII dimethylmalonate complexes with the [K(18-crown-6)]+ cationic fragments: synthesis and structure View Full Text


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Article Info

DATE

2015-03

AUTHORS

E. N. Zorina-Tikhonova, N. V. Gogoleva, A. A. Sidorov, M. A. Kiskin, I. L. Eremenko

ABSTRACT

A reaction of potassium dimethylmalonate (K2Me2Mal) with cobalt(II) or nickel(II) trimethylacetate in the presence of 18-crown-6 leads to the formation of 36-nuclear complexes {[K(18-crown-6)]2[K(H2O)(18-crown-6)]2[K6Co36(H2O)20(OH)18(Me2Mal)30(18-crown6)2(O)2]•xH2O}n (2) and {[K(H2O)2(18-crown-6)]6[K5Ni36(H2O)20(OH)18(18-crown-6)2(Me2Mal)28(HMe2Mal)2]4[K5Ni36(H2O)20(OH)20(18-crown-6)2(Me2Mal)29(HMe2Mal)]• •80H2O}n (3) (Me2Mal2– is the dianion of dimethylmalonic acid), respectively. The single crystal X-ray diffraction studies showed that the spherical 36-nuclear polyanions [Co36(H2O)12(OH)18(Me2Mal)30(O)2]10– (in compound 2) and [Ni36(H2O)12(OH)20(Me2Mal)30–x(HMe2Mal)x]y– (in compound 3; x = 1, y = 7; x = 2, y = 6) have similar structures, with their metal cores being formed of two layers: an internal one comprising 24 metal atoms and an external containing 12 metal centers. The inner cavity of the {MII36} anions was found to include one K+ aqua cation bonded to the oxygen atoms of the carboxylate or oxo ligands. More... »

PAGES

636-641

References to SciGraph publications

Journal

TITLE

Russian Chemical Bulletin

ISSUE

3

VOLUME

64

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-015-0911-9

DOI

http://dx.doi.org/10.1007/s11172-015-0911-9

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https://app.dimensions.ai/details/publication/pub.1027228548


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35 schema:description A reaction of potassium dimethylmalonate (K2Me2Mal) with cobalt(II) or nickel(II) trimethylacetate in the presence of 18-crown-6 leads to the formation of 36-nuclear complexes {[K(18-crown-6)]2[K(H2O)(18-crown-6)]2[K6Co36(H2O)20(OH)18(Me2Mal)30(18-crown6)2(O)2]•xH2O}n (2) and {[K(H2O)2(18-crown-6)]6[K5Ni36(H2O)20(OH)18(18-crown-6)2(Me2Mal)28(HMe2Mal)2]4[K5Ni36(H2O)20(OH)20(18-crown-6)2(Me2Mal)29(HMe2Mal)]• •80H2O}n (3) (Me2Mal2– is the dianion of dimethylmalonic acid), respectively. The single crystal X-ray diffraction studies showed that the spherical 36-nuclear polyanions [Co36(H2O)12(OH)18(Me2Mal)30(O)2]10– (in compound 2) and [Ni36(H2O)12(OH)20(Me2Mal)30–x(HMe2Mal)x]y– (in compound 3; x = 1, y = 7; x = 2, y = 6) have similar structures, with their metal cores being formed of two layers: an internal one comprising 24 metal atoms and an external containing 12 metal centers. The inner cavity of the {MII36} anions was found to include one K+ aqua cation bonded to the oxygen atoms of the carboxylate or oxo ligands.
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