N-nitroimidoyl chlorides: synthesis and structure View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2015-02

AUTHORS

O. V. Anikin, M. S. Klenov, A. M. Churakov, I. V. Anan´yev, K. A. Lyssenko, Yu. A. Strelenko, V. A. Tartakovsky

ABSTRACT

A new method was developed for the synthesis of N-nitroimidoyl chlorides O2N—N=C(R)Cl (R = SMe, Phth; Phth is phthalimide) by the reaction of O2N—N=C(R)SMe with SO2Cl2. The reaction of O2N—N=C(SMe)Cl with potassium phthalimide leads to the replacement of the Cl atom by the phthalimide moiety. The compounds O2N—N=C(Phth)Cl and O2N—N=C(Phth)SMe were studied by X-ray diffraction and quantum chemical methods. The C=N—N and NO2 groups in the O2N—N=C(Phth)Cl molecule were found to be completely orthogonal to each other. The explanation of this fact was proposed. More... »

PAGES

359-365

Journal

TITLE

Russian Chemical Bulletin

ISSUE

2

VOLUME

64

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-015-0869-7

DOI

http://dx.doi.org/10.1007/s11172-015-0869-7

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1054523760


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