Synthesis and structure of 2-(4′-oxo-3H-quinazolin-2′-yl)-1,3-tropolone View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-06

AUTHORS

Yu. A. Sayapin, E. A. Gusakov, A. A. Kolodina, V. N. Komissarov, I. V. Dorogan, V. V. Tkachev, G. V. Shilov, E. V. Nosova, S. M. Aldoshin, V. N. Charushin, V. I. Minkin

ABSTRACT

The acid-catalyzed condensation of 2-methyl-4-oxo-3H-quinazolin with 3,5-di(tert-butyl)-1,2-benzoquinone affords 5,7-di(tert-butyl)-2-(4′-oxo-3H-quinazolin-2′-yl)-1,3-tropolone and 2-(3,5-di(tert-butyl)-2-hydroxybenzoyl)-3H-quinazolin-4-one. The molecular structures of 5,7-di(tert-butyl)-2-(4′-oxo-3H-quinazolin-2′-yl)-1,3-tropolone and 2-(3,5-di(tert-butyl)-2-hydroxybenzoyl)-3H-quinazolin-4-one were studied by X-ray diffraction, two-dimensional NMR spectroscopy, and the density functional theory (PBE0/6-311+G**).

PAGES

1364-1372

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-014-0604-9

DOI

http://dx.doi.org/10.1007/s11172-014-0604-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1024370611


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