Synthesis of new charge-compensated cobalt bis(1,2-dicarbollide) derivatives View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-08

AUTHORS

I. D. Kosenko, I. A. Lobanova, Z. A. Starikova, V. I. Bregadze

ABSTRACT

New hetero-substituted charge-compensated cobalt bis(1,2-dicarbollide) derivatives were synthesized by the reaction of 8,8′-μ-iodo-3-commo-3-cobalta-bis(1,2-dicarba-closo-dodecaborane) [8,8′-μ-I-3,3′-Co(1,2-C2B9H10)2] with 1,4-thioxane, pyridine N-oxide, and tetrahydropyran. X-ray diffraction studies showed that the 8′-iodo-8-(pyridiniumoxy)eucosahydro-1,1′,2,2′-tetracarba-3-commo-cobalta-closo-tricosaborate molecule has the gauche-conformation (the substituents are turned with respect to each other by 69.2°). The positive charge is predominantly localized on the N(Py) atom. More... »

PAGES

1914-1918

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-013-0275-y

DOI

http://dx.doi.org/10.1007/s11172-013-0275-y

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1041344686


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