Intra- and intermolecular coordination reactions in solution involving pentacoordinated fluorosilanes based on proline View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-08

AUTHORS

A. A. Nikolin, O. V. Kuznetsova, D. E. Arkhipov, E. P. Kramarova, A. G. Shipov, A. N. Egorochkin, A. A. Korlyukov, Yu. I. Baukov, Vad. V. Negrebetskii

ABSTRACT

NMR spectroscopy was used to study a series of C,O-monochelate N′-(fluorodimethyl-silylmethyl)-N′-methyl-N-(organosulfonyl)proline amides in the solid state and in solutions in chloroform, pyridine, and acetone. The structure of one of the complexes was established by X-ray crystallography. Quantum chemical calculations were performed to interpret the spectral data obtained. The molecular conformation observed in crystal was found to be retained in solutions. The coordination bonds of silicon atom with acetone and pyridine are very weak and cannot stabilize the acyclic form (without the Si-O coordination bond). The 29Si chemical shift was found to be directly dependent on the Si-O bond distance. The mutual influence of organosulfonyl group and chelate ring was described in terms of polarization effects. More... »

PAGES

1892-1899

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-013-0272-1

DOI

http://dx.doi.org/10.1007/s11172-013-0272-1

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1046266559


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177 grid-institutes:grid.465286.b schema:alternateName G. A. Razuvaev Institute of Organometallic Chemistry, Russian Academy of Sciences, 49 ul. Tropinina, 603950, Nizhny Novgorod, Russian Federation
178 schema:name G. A. Razuvaev Institute of Organometallic Chemistry, Russian Academy of Sciences, 49 ul. Tropinina, 603950, Nizhny Novgorod, Russian Federation
179 rdf:type schema:Organization
180 grid-institutes:grid.78028.35 schema:alternateName N. I. Pirogov Russian National Research Medical University, 1 ul. Ostrovityanova, 117869, Moscow, Russian Federation
181 schema:name N. I. Pirogov Russian National Research Medical University, 1 ul. Ostrovityanova, 117869, Moscow, Russian Federation
182 rdf:type schema:Organization
 




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