Complexation of trimeric copper(i) and silver(i) 3,5-bis(trifluoromethyl)pyrazolates with amine-borane View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-08

AUTHORS

A. A. Titov, E. A. Guseva, A. F. Smol’yakov, F. M. Dolgushin, O. A. Filippov, I. E. Golub, A. I. Krylova, G. M. Babakhina, L. M. Epstein, E. S. Shubina

ABSTRACT

A complexation of trimeric copper(i) and silver(i) 3,5-bis(trifluoromethyl)pyrazolates ((ML)3) with BH3NEt3 was studied by IR spectroscopy in hexane and dichloromethane solutions. In hexane, two complexes [(ML)3][BH3NEt3]2 (1) and [(ML)3][BH3NEt3] (2) were formed depending on the ratio of reagents. In dichloromethane, only one complex [(ML)3][BH3NEt3] (2) was found. The thermodynamic parameters (ΔH○, ΔS○) of complex 1 in hexane and complex 2 in dichloromethane were obtained. The complex [(AgL)3][BH3NEt3] was isolated in the solid state, its structure was established by X-ray diffraction. The complex is formed due to two bridges B-H-Ag, one BH group is not involved in the complexation. In crystal, molecules 2 form supramolecular dimers due to the intermolecular interactions between metals of two macrocycles. More... »

PAGES

1829-1834

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-013-0263-2

DOI

http://dx.doi.org/10.1007/s11172-013-0263-2

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