Synthesis and structure of 2,2′-diaminodiphenylditelluride bis-imines View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-08

AUTHORS

I. S. Vasil’chenko, I. G. Borodkina, A. S. Burlov, N. V. Karpova, G. M. Abakarov, K. A. Lyssenko, G. S. Borodkin, I. E. Uflyand, A. D. Garnovskii, V. I. Minkin

ABSTRACT

Bis-imines of 2,2′-diaminodiphenylditelluride and 2-tosylamino (9a) and 2-hydroxybenzaldehyde (9b) were prepared and studied by X-ray diffraction, heteronuclear (1H, 13C, 15N, and 125Te) magnetic resonance, and quantum chemical calculations (Pbe1pbe/DGDZVP). According to the X-ray diffraction data, compound 9b in the crystal phase has nonsymmetrical structure: one of the tellurium atoms forms hypervalent bonding with the adjacent oxygen atom, while the second one is not involved in such interaction. The NMR study showed the symmetric molecular structure of imines 9a,b in DMSO-d6 with the tellurium atoms interacting hypervalently with the C=N nitrogen atoms. More... »

PAGES

1809-1814

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-013-0261-4

DOI

http://dx.doi.org/10.1007/s11172-013-0261-4

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1032824068


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