Synthesis, structure, and luminescence of the octahedral molybdenum cluster [Mo6I8(SC6F4H)6]2− View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-08

AUTHORS

M. N. Sokolov, M. A. Mikhailov, A. V. Virovets, K. A. Brylev, R. A. Bredikhin, A. M. Maksimov, V. E. Platonov, V. P. Fedin

ABSTRACT

A new thiolate cluster complex (Bu4N)2[Mo6I8(SC6F4H)6] was synthesized by the metathesis reaction of (Bu4N)2[Mo6I14] and HC6F4SAg in methylene chloride. According to the X-ray structure determination, the cluster core {Mo6I8}4+ coordinates six thiolate ligands 2,3,5,6-HC6F4S−. The Mo-Mo and Mo-I distances have their usual values. The average Mo-S distance is 2.538(4) Å, and the Mo-S-C angles range from 107 to 109°. Compound (Bu4N)2[Mo6I8(SC6F4H)6] both in solid and in solution displays a bright red microsecond luminescence, which is typical of octahedral molybdenum halide complexes. More... »

PAGES

1764-1767

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-013-0253-4

DOI

http://dx.doi.org/10.1007/s11172-013-0253-4

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https://app.dimensions.ai/details/publication/pub.1032020016


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