Photochemical arene exchange in the iron dicarbollide complex [(η-9-SMe2-7,8-C2B9H10)Fe(η-C6H6)]+ View Full Text


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Article Info

DATE

2013-05

AUTHORS

D. A. Loginov, M. M. Vinogradov, Z. A. Starikova, A. R. Kudinov

ABSTRACT

Visible light irradiation of the dicarbollide complex [(η-9-SMe2-7,8-C2B9H10)Fe(η-C6H6)]+ (2a) in the presence of the benzene derivatives in CH2Cl2/MeNO2 resulted in cations [(η-9-SMe2-7,8-C2B9H10)Fe(η-C6R6)]+ (2b-g; arene is anisole (b), toluene (c), m-xylene (d), mesitylene (e), durene (f), and hexamethylbenzene (g)) due to the arene exchange. The structures of [2g]PF6 and related tricarbollide complex [(η-1-ButNH-1,7,9-C3B8H10)Fe-(η-C6H6)]PF6 (1) were confirmed by X-ray diffraction analysis. The nature of bonding in cations 1, 2a, and [CpFe(η-C6H6)]+ was analyzed by an energy decomposition analysis. More... »

PAGES

1262-1267

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-013-0174-2

DOI

http://dx.doi.org/10.1007/s11172-013-0174-2

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