Synthesis, structure, and ESR spectra of the new heteronuclear complex {Li4(VO)2[(OOC)2C(H)Bu]4(H2O)8}·H2O View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-04

AUTHORS

E. S. Bazhina, G. G. Aleksandrov, N. N. Efimov, E. A. Ugolkova, V. V. Minin, A. A. Sidorov, V. M. Novotortsev, I. L. Eremenko

ABSTRACT

The reaction of an aqueous solution of vanadyl sulfate VOSO4·3H2O, butylmalonic acid (H2Bumal = C4H10(COOH)2), and lithium carbonate at pH ∼4–5 gave crystals of the complex Li4(VO)2(Bumal)4(H2O)8]·H2O (1). The structure of complex 1 was established by X-ray diffraction analysis. The molecule of complex 1 consists of two mononuclear bischelate dianionic units {VO(Bumal)2(H2O)} linked by four lithium ions to form the hexanuclear heterometallic {V2Li4} structure. The crystals and an ethanolic solution of compound 1 were studied by ESR spectroscopy. More... »

PAGES

962-965

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-013-0125-y

DOI

http://dx.doi.org/10.1007/s11172-013-0125-y

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1020042139


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