Interaction of the Negishi reagent Cp2ZrBun2 with 1,4-bis(tert-butyl)butadiyne View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2012-01

AUTHORS

V. V. Burlakov, V. S. Bogdanov, K. A. Lyssenko, A. Spannenberg, P. V. Petrovskii, W. Baumann, P. Arndt, M. Kh. Minacheva, B. N. Strunin, U. Rosenthal, V. B. Shur

ABSTRACT

The interaction of the Negishi reagent Cp2ZrBun2 with 1,4-bis(tert-butyl)butadiyne ButC≡C-C≡CBut leads to four products: a five-membered zirconacyclocumulene complex Cp2Zr(η4-ButC4But) (2) synthesized earlier by another method, the previously unknown seven-membered zirconacyclocumulene Cp2Zr[η4-ButC4(But)-C(C2But)=CBut] (3) as well as small amounts of the zirconocene binuclear butatrienyl complex Cp2(Bun)Zr(ButC4But)Zr(Bun)Cp2 (4), and the dimeric acetylide [Cp2ZrC≡CBut]2 (5). The structure of complexes 2–5 was established by X-ray diffraction studies. More... »

PAGES

165-173

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-012-0023-8

DOI

http://dx.doi.org/10.1007/s11172-012-0023-8

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1021316264


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