Polyadducts of fullerene C60 with tert-butyl groups View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2011-09

AUTHORS

E. A. Rychagova, L. V. Kalakutskaya, S. N. Titova, G. A. Domrachev, S. Yu. Ketkov

ABSTRACT

New soluble fullerene derivatives ButnC60 were synthesized by the reaction of C60Mn(THF)x (M = Li, Na; n = 4, 6, 8, 10, 12) with tert-butyl bromide ButBr. The thus obtained compounds were characterized by spectroscopic methods (IR and NMR spectroscopy), mass spectrometry (MALDI), elemental analysis, and quantum chemical calculations. HPLC was used for chromatographic separation of the products of the reaction of C60Nan(THF)x (n = 4, 6, 8, 12) with ButBr. It was found that But4C60 and But6C60 decompose on the column. A complex of physicochemical methods of analysis was used for establishing compositions of individual fractions of chromatographic separation of But4C60. The structure of one of the components was determined as 1-tert-butyl-1,2-dihydrofullerene 1,2-ButC60H. More... »

PAGES

1888-1898

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-011-0285-6

DOI

http://dx.doi.org/10.1007/s11172-011-0285-6

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1011110472


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