Inclusion compounds of the copper(ii) and zinc(ii) complexes with cyclam in cucurbit[8]uril: synthesis and structure View Full Text


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Article Info

DATE

2011-05

AUTHORS

E. A. Kovalenko, D. A. Mainichev, O. A. Gerasko, D. Yu. Naumov, V. P. Fedin

ABSTRACT

Inclusion compounds of the macrocyclic cavitand cucurbit[8]uril (CB[8], C48H48N32O16) with the copper(ii) and zinc(ii) complexes with the tetraazamacrocyclic ligand cyclam, {[Cu(cyclam)(H2O)2]@CB[8]}Cl2·18H2O (1) and {[Zn(cyclam)]@CB[8]}Cl2·13H2O (2), were synthesized. The compounds were characterized by X-ray diffraction analysis, electrospray mass spectrometry, IR spectroscopy, and elemental analysis. The 1H and 13C NMR method revealed only one trans-isomer of the zinc(ii) complex with cyclam in an aqueous solution of inclusion compound 2. More... »

PAGES

841-848

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URI

http://scigraph.springernature.com/pub.10.1007/s11172-011-0132-9

DOI

http://dx.doi.org/10.1007/s11172-011-0132-9

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https://app.dimensions.ai/details/publication/pub.1015115802


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