Investigation of cobalt (1,10-phenanthroline)-bis-(3,6-di-tert-butyl-o-benzosemiquinolate) by X-ray diffraction, IR and ESR spectroscopy, magnetochemistry, and precision calorimetry View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2011-03

AUTHORS

M. P. Bubnov, N. A. Skorodumova, A. S. Bogomyakov, G. V. Romanenko, A. V. Arapova, K. A. Kozhanov, N. N. Smirnova, G. A. Abakumov, V. K. Cherkasov

ABSTRACT

The bistable cobalt complex containing two symmetrical 3,6-di-tert-butyl-o-benzoquinone and one 1,10-phenanthroline moieties as ligands (1) was synthesized. Complex 1 was isolated in the individual state and characterized by IR and ESR spectroscopy, X-ray diffraction, magnetochemical studies, and precision calorimetry. A change in temperature causes the reversible metal-ligand electron transfer and spin crossover (redox isomerism) in complex 1 in the crystalline state. The redox-isomeric transformation at ∼250 K is accompanied by the phase transition. The structural study at two temperatures confirmed the changes in the molecular and crystal structure associated with the redox-isomeric transformation. More... »

PAGES

449

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-011-0071-5

DOI

http://dx.doi.org/10.1007/s11172-011-0071-5

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