Inclusion compounds of cucurbit[8]uril with noble metal polyamine complexes View Full Text


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Article Info

DATE

2010-11

AUTHORS

E. A. Kovalenko, T. V. Mitkina, O. A. Gerasko, D. Yu. Naumov, D. G. Samsonenko, V. P. Fedin

ABSTRACT

Inclusion compounds of the macrocyclic cavitand cucurbit[8]uril (CB[8]) with the ruthenium(iii) bis(ethylenediamine) complex {trans-[Ru(en)2Cl2]@CB[8]}Cl·27.5H2O (1), the gold(iii) diethylenetriamine complex {[Au(dien)Cl]@CB[8]}Cl2·11H2O (2), and the gold(iii) and platinum(ii) cyclam complexes (H3O)5{[Au(cyclam)]@CB[8]}Cl8·18H2O (3) and {[Pt(cyclam)]0.11(H2cyclam)0.89@CB[8]}Cl2·16H2O (4), respectively, where cyclam is the tetraazamacrocyclic ligand, were synthesized. The inclusion compounds were synthesized both directly starting from CB[8] and the metal complexes with polyamines (en or dien) and by the two-step method with the use of the cyclic polyamine ligand (cyclam) pre-included into the cavity of the macrocycle. The inclusion compounds were characterized by X-ray diffraction (1, 2, and 4), IR spectroscopy, electrospray ionization mass spectrometry, UV-Vis spectroscopy, and thermogravimetric analysis. More... »

PAGES

2072

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-010-0357-z

DOI

http://dx.doi.org/10.1007/s11172-010-0357-z

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https://app.dimensions.ai/details/publication/pub.1016287107


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