Reaction of 5-methyl-1,3,4-thiadiazoline-2-thione with molecular iodine View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2010-09

AUTHORS

M. S. Chernov’yants, N. V. Aleshina, Z. A. Starikova, E. N. Sul’zhenko

ABSTRACT

The formation of the n-σ* complex of 5-methyl-1,3,4-thiadiazoline-2-thione with molecular iodine of the composition C3H4N2S2·I2 in dilute chloroform solutions was studied by UV-Vis spectroscopy. The crystal and molecular structure of the new salt bis(5-methyl-1,3,4-thiadiazol-2-ylthio)iodonium pentaiodide [(C3H4N2S2)2I+]I5− was determined by X-ray diffraction. This salt is formed by the chemical reaction of thione with elemental iodine. In the crystal structure of the salt, the molecules are linked by hydrogen bonds into chains along the [011] diagonal direction. The crystalline salt is characterized by the presence of chains of dimers formed through S…S (3.587(2) Å) and I…I (4.0729(7) Å) contacts corresponding to the interactions between the sulfur atom of the heterocycle and the thione sulfur atom and between the central iodine atoms, respectively. The mixed supramolecular layers are linked by short contacts between the thione sulfur atoms (3.645(3) Å). The behavior of 5-methyl-1,3,4-thiadi-azoline-2-thione, which is a potential antithyroid drug, toward molecular iodine was investigated. More... »

PAGES

1797-1802

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-010-0315-9

DOI

http://dx.doi.org/10.1007/s11172-010-0315-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1038938933


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