Photochemical replacement of benzene in the tetramethylcyclopentadienyl complex of iron, [η-C5Me4H)Fe(η-C6H6)]+ View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2010-07

AUTHORS

D. A. Loginov, I. D. Baravi, O. I. Artyushin, Z. A. Starikova, P. V. Petrovskii, A. R. Kudinov

ABSTRACT

Irradiation of the cation [η-C5Me4H)Fe(η-C6H6)]++ (1) and ButNC with visible light in acetonitrile results in the displacement of the benzene ligand, giving [(η-C5Me4H)Fe(ButNC)3]+ (2). Reactions of complex 1 with P(OR)3 and dppe in MeCN yield the complexes [(η-C5Me4H)-Fe(MeCN)P(OR)32]+ (R = Me (3) and Et (4)) and [(η-C5Me4H)Fe(MeCN)(dppe)]+ (5) containing two Fe—P bonds. The same reactions in CH2Cl2 give the tris(phosphite) complexes [(η-C5Me4H)FeP(OR)33]+ (6, 7). A photochemical reaction of complex 1 with pentaphos-phaferrocene Cp*Fe(η-cyclo-P5) yields the triple-decker cation [(η-C5Me4H)Fe(μ-η:η-cyclo-P5)FeCp*]+ (8) with a bridging pentaphospholyl ligand. Structures [2]PF6 and [3]PF6 were identified by X-ray diffraction. More... »

PAGES

1312-1316

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-010-0240-y

DOI

http://dx.doi.org/10.1007/s11172-010-0240-y

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1007974904


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