Formation of polynuclear architectures with copper atoms and 1,1-cyclohexanediacetate anions View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2010-06

AUTHORS

N. V. Zauzolkova, M. E. Nikiforova, A. A. Sidorov, I. A. Apolonskaya, M. V. Fedin, V. V. Minin, A. V. Rotov, E. A. Ugolkova, M. A. Kiskin, G. G. Aleksandrov, V. M. Novotortsev, I. L. Eremenko

ABSTRACT

The reaction of copper nitrate Cu(NO3)2·3H2O with potassium salt of 1,1-cyclohexanediacetic acid (H2CHDAA) in an EtOH-toluene mixture affords the polymeric complex {[(EtOH)2Cu2(CHDAA)2]·EtOHn (1). The addition of pyridine to the Cu(NO3)2·3H2O-K2CHDAA reaction system in an EtOH-MeCN mixture results in the isolation of the unusual octadecanuclear heterometallic cluster [K2(η1-H2O)6(η1-py)8Cu16-(η1-OH)2(μ4-CHDAA)16]·EtOH·MeCN·3H2O (2). In complex 2, the hexadecanuclear metal carboxylate dianion (η1-H2O)6(η1-py)8Cu16(η1-OH)2(μ4-CHDAA)16 acts as the metal-containing macropolycyclic ligand. The newly synthesized compounds 1 and 2 were characterized by X-ray diffraction and EPR. More... »

PAGES

1186-1191

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-010-0221-1

DOI

http://dx.doi.org/10.1007/s11172-010-0221-1

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https://app.dimensions.ai/details/publication/pub.1051057503


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