Synthesis, crystal structure, and interconversions of new N-aryl-1,3,5-dithiazinanes, 1,3,5-thiadiazinanes, and 1,5-dithia-3,7-diazacyclooctanes View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2010-05

AUTHORS

V. R. Akhmetova, Z. T. Niatshina, G. R. Khabibullina, I. S. Bushmarinov, A. O. Borisova, Z. A. Starikova, L. F. Korzhova, R. V. Kunakova

ABSTRACT

Chemoselectivity of multicomponent reaction of anilines with the CH2O-H2S thiomethylating mixture in the synthesis of N-aryl-substituted 1,3,5-dithiazinanes, 1,3,5-thiadiazinanes, and 1,5-dithia-3,7-diazacyclooctanes has been studied depending on the type and mutual arrangement of substituents in the starting anilines, ratio of reagents, temperature, and reaction time. Conformation of the synthesized heterocycles in crystal has been found by X-ray diffraction. Interconversion of the heterocycles showed stability of N-aryl-1,3,5-dithiazinanes. More... »

PAGES

1002-1009

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-010-0196-y

DOI

http://dx.doi.org/10.1007/s11172-010-0196-y

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1001245055


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