Synthesis and structure of novel chiral amido-imine complexes of aluminum, gallium, and indium View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2009-11

AUTHORS

A. N. Tishkina, A. N. Lukoyanov, A. G. Morozov, G. K. Fukin, K. A. Lyssenko, I. L. Fedushkin

ABSTRACT

The reactions of 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene (dpp-BIAN, 1) with tri-iso-butylaluminum, triethylgallium or trimethylindium give the novel amido-imine complexes (Bui—dpp-BIAN)AlBui2 (4), (Et—dpp-BIAN)GaEt2 (5), and (Me—dpp-BIAN)InMe2 (6), respectively. The reaction of (dpp-BIAN)AlI(Et2O) (7) with allyl bromide affords analogous chiral amido-imine derivative (All—dpp-BIAN)AlBrI (8). Hydrolysis of 8 affords the amino-imino compound (All—dpp-BIAN)H (9). The new compounds 4–6, 8, and 9 have been characterized by 1H NMR and IR spectroscopy. The molecular structures of 5, 6, and 9 were determined by single crystal X-ray analysis. More... »

PAGES

2250-2257

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-009-0314-x

DOI

http://dx.doi.org/10.1007/s11172-009-0314-x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1012408127


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