Dinuclear chelates of acyclic and cyclic tridentate Schiff bases derived from sterically hindered o-aminophenols. A new type of reactivity of ... View Full Text


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Article Info

DATE

2009-07

AUTHORS

T. O. Shmakova, D. A. Garnovskii, K. A. Lyssenko, E. P. Ivakhnenko, V. V. Krasnikov, V. I. Simakov, I. S. Vasil’chenko, A. I. Uraev, A. S. Burlov, E. V. Sennikova, A. S. Bogomyakov, M. Yu. Antipin, A. D. Garnovskii, I. E. Uflyand

ABSTRACT

The chemical and electrochemical synthesis of cobalt(II), nickel(II), and copper(II) complexes based on sterically hindered tridentate Schiff bases obtained by the coupling of 2-amino-4,6-di-tert-butylphenol with salicylaldehyde derivatives (H2L, H2L’) was performed. The resulting dinuclear complexes were characterized by elemental analysis, IR spectroscopy, and magnetochemical measurements in the 300–2 K temperature range. The structures of the dinuclear nickel(II) and copper(II) complexes with the composition Ni2L2·2AcOH·2MeOH and Cu2L2, respectively, were established by X-ray diffraction. The copper chelates are characterized by the presence of antiferromagnetic exchange interactions. The mononuclear copper(II) complexes (DMSO)bis[2-(5,7-di-tert-butyl-4-hydroxybenzoxazol-2-yl)phenolato]copper(II) and (DMF)2bis[2-(5,7-di-tert-butyl-4-hydroxybenzoxazol-2-yl)phenolato]copper(II) were isolated upon electrochemical dissolution of copper(0) and were structurally characterized. More... »

PAGES

1383-1391

References to SciGraph publications

  • 2006-12. Luminescent complexes with ligands containing C=N bond in RUSSIAN JOURNAL OF COORDINATION CHEMISTRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s11172-009-0184-2

    DOI

    http://dx.doi.org/10.1007/s11172-009-0184-2

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1011288955


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    Download the RDF metadata as:  json-ld nt turtle xml License info

    HOW TO GET THIS DATA PROGRAMMATICALLY:

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    N-Triples is a line-based linked data format ideal for batch operations.

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    RDF/XML is a standard XML format for linked data.

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