Synthesis and structures of dinuclear ZrIV and HfIV hydroxo complexes with the monolacunar Keggin and Dawson anions View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2009-03

AUTHORS

M. N. Sokolov, N. V. Izarova, E. V. Peresypkina, A. V. Virovets, V. P. Fedin

ABSTRACT

The reactions of the tetranuclear hydroxo complexes [M4(fu2-OH)8(H20)16]8+ (M = Zr or Hf) with monolacunar Keggin-type [α-PW11O39]7- and Dawson-type [α2-P2W17O61] phosphotungstates afford the polyoxoanions [(H2O)HT(fu2-OH)(PW11O39)2]8- and [(H2O)M(fu2-OH)(P2W17O61)2]14- (M = Zr or Hf), respectively, in which the 1: 1 heterometal lacunary polyoxotungstate complexes are linked into dimers through two hydroxo bridges coordinated to the heterometal atoms. The structures of these compounds were established by single-crystal X-ray diffraction and confirmed by 31P NMR spectroscopy in solution. More... »

PAGES

507-512

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-009-0048-9

DOI

http://dx.doi.org/10.1007/s11172-009-0048-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1008054847


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