Coordination chemistry of anticrowns. Complexation of cyclic trimeric perfluoro-o-phenylenemercury (o-C6F4Hg)3 with the cyanoborohydride anion [H3BCN]− and triethylamineborane Et3NBH3 View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2008-12

AUTHORS

V. N. Tsupreva, O. A. Filippov, F. M. Dolgushin, K. I. Tugashov, A. I. Krylova, V. I. Bragin, I. A. Tikhonova, V. B. Shur, L. M. Epstein, E. S. Shubina

ABSTRACT

As was shown by IR spectroscopy, the reaction of the three-mercury anticrown (o-C6F4Hg)3 (1) with the [H3BCN]ion in THF affords the complexes {[(o-C6F4Hg)3][H3BCN](5) and [(o-C6F4Hg)3]2[H3BCN](6). Complex 6 was isolated from solution in the analytically pure state. According to X-ray diffraction data, complex 6 has a double-decker sandwich structure, in which the borohydride group of the [H3BCN]− anion is bound to one anticrown molecule by three B-H-Hg bridges, whereas the cyanide group is cooperatively coordinated by three mercury centers of another molecule 1 through the nitrogen atom. The reaction of compound 1 with triethylamineborane Et3NBH3 in THF affords the 1: 1 complex ∼[(o-C6F4Hg)3][Et3NBH3]∼ (7). In this adduct, the binding of the aminoborane to the mercury anticrown is also accomplished by B-H-Hg bridges. The stability constants of complexes 5 and 6 in THF were determined. More... »

PAGES

2540-2547

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-008-0365-4

DOI

http://dx.doi.org/10.1007/s11172-008-0365-4

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1036919159


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