Ruthenium complexes with ferrocene-based P,C,P pincer ligand View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2007-09

AUTHORS

A. M. Sheloumov, F. M. Dolgushin, M. V. Kondrashov, P. V. Petrovskii, Kh. A. Barbakadze, O. I. Lekashvili, A. A. Koridze

ABSTRACT

First ruthenium complexes with a ferrocene-based pincer ligand were synthesized. The cyclometallation of 1,3-bis[(di-tert-butylphosphino)methyl]ferrocene with RuCl2(DMSO)4 in 2-methoxyethanol afforded the RuCl(CO)[{2,5-(But2PCH2)2C5H2}Fe(C5H5)](RuCl(CO)\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document} $$[^{Bu^t } P,C,P^{Fe} ]$$ \end{document}) complex (5). Complex 5 reversibly binds CO to form the RuCl(CO)2\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document} $$[^{Bu^t } P,C,P^{Fe} ]$$ \end{document} complex (6). The analogous reaction in the presence of NaBAr′4 (Ar′ = 3,5-(CF3)2C6H3) produced the cationic complex {Ru(CO)2\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document} $$[^{Bu^t } P,C,P^{Fe} ]$$ \end{document}}BAr′4 (7). The structures of complexes 5 and 7 were established by single-crystal X-ray diffraction. The X-ray diffraction study revealed an agostic interaction between one of the C-H bonds of the axial (exo-oriented with respect to the ferrocene iron atom) tert-butyl group and the Ru atom in complexes 5 and 7. More... »

PAGES

1757-1764

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-007-0273-z

DOI

http://dx.doi.org/10.1007/s11172-007-0273-z

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1005350880


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