Replacement of carboxylate bridges in polynuclear nickel pivalates with 2-hydroxy-6-methylpyridine anions View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2007-05

AUTHORS

M. E. Nikiforova, A. A. Sidorov, G. G. Aleksandrov, V. N. Ikorskii, I. V. Smolyaninov, A. O. Okhlobystin, N. T. Berberova, I. L. Eremenko

ABSTRACT

The reaction of 2-hydroxy-6-methylpyridine (HL, 1) with nonanuclear nickel trimethyl-acetate Ni9(OH)6(OOCCMe3)12(HOOCCMe3)4 (2) in MeCN with a ratio M: L = 1: 1 under mild conditions (20 °C, 15 min) led to degradation of the metal core to form the hexanuclear complex (HL)2(µ 2-HL)2Ni6(µ3-OH)2(µ2-H2O)2(µ-OOCCMe3)8(η-OOCCMe3)2 (3). Further heating of 3 in acetonitrile at 80 °C for 4 h afforded the (HL)Ni6(µ 3-OH)(µ3,η2-L)3(µ,η2-L)(µ3-L)(µ 3-OOCCMe3)(µ-OOCCMe3)4(η2-OOCCMe3) complex. The reaction with the use of a 2: 1 THF-EtOH mixture instead of acetonitrile at 50 °C gave the decanuclear complex [Ni10(µ 3-O)2(µ3-OH)4(µ-OOCCMe3)6(µ3,η 2-L)6(EtOH)6](H2O)2, which is also produced from compounds 1 and 2 in ethanol. The structures of the resulting complexes were established by X-ray diffraction. More... »

PAGES

943-952

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11172-007-0143-8

DOI

http://dx.doi.org/10.1007/s11172-007-0143-8

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https://app.dimensions.ai/details/publication/pub.1004103994


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