Structural and textural features of TiO2/SAPO-34 nanocomposite prepared by the sol–gel method View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2016-12

AUTHORS

Salima Bellatreche, Abdelkrim Hasnaoui, Bouhadjar Boukoussa, Jaime García-Aguilar, Ángel Berenguer-Murcia, Diego Cazorla-Amoros, Abdelkader Bengueddach

ABSTRACT

This paper focuses on the synthesis of nanocomposite materials, TiO2/SAPO-34, using the sol–gel method, which involves preparing a mixture between as-synthesized or calcined SAPO-34 zeolite and TiO2 gel under hydrothermal crystallization and then calcining it at 400 °C for the formation of the TiO2 anatase phase. The structural and textural features of the obtained materials were determined by various physico-chemical techniques such as thermogravimetric analysis, X-ray diffraction, scanning electronic microscopy, nitrogen sorption at 77 K, energy dispersive X-ray analysis and ultraviolet–visible spectrometry. The DRX results showed that calcination at 400 °C of the mixture between the calcined SAPO-34 and TiO2 gel led to the collapse of the original framework of zeolite, but formed the anatase TiO2 in a nano-spherical morphology; however, the use of as-synthesized SAPO-34 supports provides a mixture phase between SAPO-34 and TiO2 anatase after calcination. The photocatalytic properties of the SAPO-34/TiO2 and TiO2-type materials were tested for the removal of methylene blue (MB) dye. The MB degradation proved to increase as a function of contact time, catalyst mass and the initial concentration of MB. More... »

PAGES

8039-8053

References to SciGraph publications

  • 2012-03. Phase transition at thermal dehydration in stilbite in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
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    http://scigraph.springernature.com/pub.10.1007/s11164-016-2577-9

    DOI

    http://dx.doi.org/10.1007/s11164-016-2577-9

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    https://app.dimensions.ai/details/publication/pub.1029530979


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