Mechanochemically modified hydrazine reduction method for the synthesis of nickel nanoparticles and their catalytic activities in the Suzuki–Miyaura cross-coupling reaction View Full Text


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Article Info

DATE

2019-04

AUTHORS

Katalin Musza, Márton Szabados, Adél Anna Ádám, Zoltán Kónya, Ákos Kukovecz, Pál Sipos, István Pálinkó

ABSTRACT

The commonly used hydrazine reduction method for the synthesis of Ni nanoparticles was integrated with the mechanochemical treatment of the nickel hydroxide precursors to modify the structural and catalytic attributes of the as-prepared metallic nickel materials. The precursors and the nanoparticles were studied by X-ray diffractometry, infrared spectroscopy, and dynamic light scattering as well as scanning electron microscopy. The changes in catalytic activities were followed in the Suzuki–Miyaura cross-coupling reaction between iodobenzene and phenylboronic acid and correlated with structural changes resulting from mechanochemical pretreatment. More... »

PAGES

1-12

References to SciGraph publications

  • 2014-07. Preparation of NiO nanoparticles from Ni(OH)2·NiCO3·4H2O precursor by mechanical activation in INTERNATIONAL JOURNAL OF MINERALS, METALLURGY, AND MATERIALS
  • 2008-03. Biosynthesis of nanoparticles: technological concepts and future applications in JOURNAL OF NANOPARTICLE RESEARCH
  • 2006-01. Effects of ball milling on the physical and electrochemical characteristics of nickel hydroxide powder in JOURNAL OF APPLIED ELECTROCHEMISTRY
  • 2004-08. Mechanochemical synthesis of nanoparticles in JOURNAL OF MATERIALS SCIENCE
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    http://scigraph.springernature.com/pub.10.1007/s11144-018-1509-7

    DOI

    http://dx.doi.org/10.1007/s11144-018-1509-7

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    https://app.dimensions.ai/details/publication/pub.1110281571


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