Iron-containing materials as catalysts for the synthesis of 1,5-benzodiazepine from 1,2-phenylenediamine and acetone View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-08

AUTHORS

Maria N. Timofeeva, Sergey A. Prikhod’ko, Kristina N. Makarova, Mikhail E. Malyshev, Valentina N. Panchenko, Artem B. Ayupov, Sung Hwa Jhung

ABSTRACT

The cyclocondensation of 1,2-phenylenediamine (I) with acetone was investigated in the presence of Fe-containing microporous nickel phosphate molecular sieves (Fe-VSB-5) and Fe-containing mesoporous mesophase materials (Fe-MMM). The main product was 2,3-dihydro-2,2,4-trimethyl-1H-1,5-benzodiazepine (1,5-benzodiazepine) with 86–88% yield at 50 °C, with an acetone/(I) molar ratio of 2.5 in methanol as the reaction medium. The Fe content was found to affect not only the reaction rate but also yield of 1,5-benzodiazepine. The high reaction rate and yield of 1,5-benzodiazepine were—achieved with isolated iron sites in frameworks of Fe-VSB-5 and Fe-MMM. More... »

PAGES

689-699

References to SciGraph publications

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URI

http://scigraph.springernature.com/pub.10.1007/s11144-017-1190-2

DOI

http://dx.doi.org/10.1007/s11144-017-1190-2

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https://app.dimensions.ai/details/publication/pub.1085093586


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