Ontology type: schema:ScholarlyArticle
2005-05
AUTHORSI. A. Charushnikova, N. N. Krot, I. N. Polyakova, V. I. Makarenkov
ABSTRACTDouble U(VI) phthalates with NH4+, K+, and Cs+ ions in the outer sphere were synthesized. The X-ray phase analysis shows that their structures are similar. Single crystals were prepared and the structure of K4[(UO2)4(μ3-O)2(C6H4C2O4)4] ⋅ 3H2O was solved. In the [(UO2)4O2(C6H4C2O4)4]4− anions forming the main structural motif, each bridging oxygen atom μ3-O combines one pentagonal and two hexagonal bipyramids, which, in turn, are combined in centrosymmetrical tetramers. The phthalate ions have coordination capacity equal to 3; each ligand coordinates U(1) in the bidentate fashion via one carboxy group and U(2) in the bidentate fashion to form a planar seven-membered chelate ring. More... »
PAGES241-246
http://scigraph.springernature.com/pub.10.1007/s11137-005-0080-z
DOIhttp://dx.doi.org/10.1007/s11137-005-0080-z
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