Combustion synthesis of silicon nitride using ultrafine silicon powders View Full Text


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Article Info

DATE

2009-07

AUTHORS

V. V. Zakorzhevskii, I. P. Borovinskaya

ABSTRACT

The paper examines the synthesis of α-Si3N4 using ultrafine powders of silicon and inert diluent (α-Si3N4). It is established that the combustion temperature of the mixture based on silicon particles 200 nm in diameter is lower than the silicon melting point (1420°C). The low combustion temperature is obviously attributed to a nanofraction in the silicon powder. The specific surface area of silicon nitride increases with decreasing silicon fraction in the starting mixture. When Si with Ssp = 6 m2/g and 12 m2/g is used, the maximum specific surface area of Si3N4 is 6.5 m2/g and 9.6 m2/g, respectively. The content of the low-temperature Si3N4 (alpha phase) modification remains the same in the synthesis product: α /(α + β) ⋅ 100% = 89–93% (∼95 wt.%). More... »

PAGES

375-380

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11106-009-9155-2

DOI

http://dx.doi.org/10.1007/s11106-009-9155-2

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1036403622


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