The Atropomer Composition of Iopromide as an Indicator for Assessment of the Quality of its Substance and Medincal Formulations View Full Text


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Article Info

DATE

2014-06

AUTHORS

R. G. Glushkov*, M. S. Goizman, D. A. Arantseva, N. N. Demidova, E. K. Kulaeva, M. B. Zagudailova, D. E. Dmitriev, A. S. Trifilenkov, A. A. Korlyukov, D. E. Arkhipov, K. Yu. Suponitskii, N. L. Shimanovskii, S. A. Zaitsev, E. V. Degterev

ABSTRACT

The atropisomer composition of iopromide substance and formulations is discussed. At 120 °C in aqueous iopromide solution, its atropisomers were found to be converted to conformers, which reached equilibrium with each other in 15 min at this temperature. Thus, the atropisomer composition of iopromide substance in solutions prepared using the technical method as described inevitably consists of the equilibrium between conformers formed at 120 °C. The equilibrium composition of these solutions persists after cooling, i.e., after return of conformers to the state of atropisomers. The relative content of the E1 and E2 (USP terminology) atropisomers (ΣE) is an important quality indicator for iopromide formulations; only compliance with the inequality ΣE ≥ 20 % guarantees phase stability of solutions with working concentrations of iopromide ( ≤ 769 mg/ml) over a wide range of temperatures (0 – 120 °C). The inequality ΣE ≥ 20 % is inevitably reached during heat sterilization of iopromide. More... »

PAGES

186-195

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11094-014-1075-x

DOI

http://dx.doi.org/10.1007/s11094-014-1075-x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1033174408


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