A comprehensive investigation on electrophoretic self-assembled nano-Co3O4 films in aqueous solution as electrode materials for supercapacitors View Full Text


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Article Info

DATE

2016-06

AUTHORS

Xiaogang Guo, Xueming Li, Zhongshu Xiong, Chuan Lai, Yu Li, Xinyue Huang, Hebin Bao, Yanjun Yin, Yuhua Zhu, Daixiong Zhang

ABSTRACT

In this study, the nano-Co3O4 films (NCOFs) have been prepared by a one-step cathodic electrophoretic deposition (C-EPD) in aqueous solutions with micro-additive polyethylenimine at ambient temperature and pressure for oxide film-based supercapacitors. The phase composition and morphology of the NCOFs were studied by X-ray diffraction (XRD) and focused ion beam scanning electron microscope (FIB-SEM), respectively. In addition, the deposition kinetics of nano-Co3O4 particles using C-EPD process were investigated in detail. The electrochemical capacitance behaviors of the NCOFs electrode were analyzed by cyclic voltammetry, galvanostatic charge–discharge studies, and electrochemical impedance spectroscopy in 2 M KOH solution. The electrochemical experiments revealed that the highest capacitance of 233.6 F g−1 at 0.5 A g−1, 93.5 % of which still be maintained after 2000 charge–discharge cycles. These findings suggested the potential application of the NCOFs prepared by C-EPD in the electrochemical supercapacitors. More... »

PAGES

144

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11051-016-3456-4

DOI

http://dx.doi.org/10.1007/s11051-016-3456-4

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1043693789


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39 schema:description In this study, the nano-Co3O4 films (NCOFs) have been prepared by a one-step cathodic electrophoretic deposition (C-EPD) in aqueous solutions with micro-additive polyethylenimine at ambient temperature and pressure for oxide film-based supercapacitors. The phase composition and morphology of the NCOFs were studied by X-ray diffraction (XRD) and focused ion beam scanning electron microscope (FIB-SEM), respectively. In addition, the deposition kinetics of nano-Co3O4 particles using C-EPD process were investigated in detail. The electrochemical capacitance behaviors of the NCOFs electrode were analyzed by cyclic voltammetry, galvanostatic charge–discharge studies, and electrochemical impedance spectroscopy in 2 M KOH solution. The electrochemical experiments revealed that the highest capacitance of 233.6 F g−1 at 0.5 A g−1, 93.5 % of which still be maintained after 2000 charge–discharge cycles. These findings suggested the potential application of the NCOFs prepared by C-EPD in the electrochemical supercapacitors.
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