The impact of the chemical synthesis on the magnetic properties of intermetallic PdFe nanoparticles View Full Text


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Article Info

DATE

2015-05-22

AUTHORS

I. Castellanos-Rubio, M. Insausti, I. Gil de Muro, D. Carolina Arias-Duque, Juan Carlos Hernández-Garrido, T. Rojo, L. Lezama

ABSTRACT

Palladium-rich Iron nanoparticles in the 4–8 nm range have been produced by a combination of two methods: the thermal decomposition of organometallic precursors and the reduction of metallic salts by a polyol. Herein, it is shown how the details of the synthesis have a striking impact on the magnetic and morphological properties of the final products. In the synthesis of these bimetallic nanoparticles, the use of high reaction temperatures plays an essential role in attaining good chemical homogeneity, which has proved to have a key influence on the magnetic properties. Magnetic characterization has been performed by electron magnetic resonance and magnetization measurements, which have confirmed the superparamagnetic-like behavior at room temperature. No clear traces of magnetic polarization in palladium atoms have been detected. The combination of long-term stability and homogeneous chemical and magnetic properties makes these particles very suitable for a wide range of applications in nanotechnology. More... »

PAGES

229

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11051-015-3042-1

DOI

http://dx.doi.org/10.1007/s11051-015-3042-1

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187 grid-institutes:grid.11480.3c schema:alternateName Dpto. de Química Inorgánica, Universidad del País Vasco, UPV/EHU, P.O. Box 644, 48080, Bilbao, Spain
188 schema:name Dpto. de Química Inorgánica, Universidad del País Vasco, UPV/EHU, P.O. Box 644, 48080, Bilbao, Spain
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190 grid-institutes:grid.424082.8 schema:alternateName CIC EnergiGUNE, Parque Tecnológico de Álava, Albert Einstein 48, ED. CIC, 01510, Miñano, Spain
191 schema:name CIC EnergiGUNE, Parque Tecnológico de Álava, Albert Einstein 48, ED. CIC, 01510, Miñano, Spain
192 Dpto. de Química Inorgánica, Universidad del País Vasco, UPV/EHU, P.O. Box 644, 48080, Bilbao, Spain
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194 grid-institutes:grid.7759.c schema:alternateName Departamento de Ciencia de los Materiales e Ingeniería Metalúrgica y Química Inorgánica, Facultad de Ciencias, Universidad de Cadiz, Apartado 40, Puerto Real, 11510, Cadiz, Spain
195 schema:name Departamento de Ciencia de los Materiales e Ingeniería Metalúrgica y Química Inorgánica, Facultad de Ciencias, Universidad de Cadiz, Apartado 40, Puerto Real, 11510, Cadiz, Spain
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