Preparation of size-tunable, highly monodisperse PVP-protected Pt-nanoparticles by seed-mediated growth View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2008-08

AUTHORS

Matthias M. Koebel, Louis C. Jones, Gabor A. Somorjai

ABSTRACT

We demonstrate a preparative method which produces highly monodisperse Pt-nanoparticles of tunable size without the external addition of seed particles. Hexachloroplatinic acid is dosed slowly to an ethylene glycol solution at 120 °C and reduced in the presence of a stabilizing polymer poly-N-vinylpyrrolidone (PVP). Slow addition of the Pt-salt will first lead to the formation of nuclei (seeds) which then grow further to produce larger particles of any desired size between 3 and 8 nm. The amount of added hexachloroplatinic acid precursor controls the size of the final nanoparticle product. TEM was used to determine size and morphology and to confirm the crystalline nature of the nanoparticles. Good reproducibility of the technique was demonstrated. Above 7 nm, the particle shape and morphology changes suddenly indicating a change in the deposition selectivity of the Pt-precursor from (100) towards (111) crystal faces and breaking up of larger particles into smaller entities. More... »

PAGES

1063-1069

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11051-008-9370-7

DOI

http://dx.doi.org/10.1007/s11051-008-9370-7

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1052257093


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