Rh(I)/Sc(OTf)3-co-catalyzed Michael addition of ammonium ylide to (E)-1,4-enediones: synthesis of functionalized 1,4-diketones. View Full Text


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Article Info

DATE

2019-04-05

AUTHORS

Qinghua Wei, Zi Li, Xi Yang, Jianghui Chen, Xiaohua Liu, Wenhao Hu, Shunying Liu

ABSTRACT

A Rh(I)/Sc(III) co-catalyzed synthesis of highly valuable functionalized 1,4-diketone derivatives in good yields and with an excellent diastereoselectivity. The established method provides a rapid approach to structurally diverse 1,4-diketone scaffold in a very mild and rapid fashion from simple starting materials. Moreover, the protocol could be easily scaled up to gram-scale synthesis. An attempt to develop an asymmetric version of the Rh(I)/guanidine system was also explored, resulting in a moderate enantioselectivity (71% ee). More... »

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11030-019-09941-8

DOI

http://dx.doi.org/10.1007/s11030-019-09941-8

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1113261890

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30953296


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51 schema:description A Rh(I)/Sc(III) co-catalyzed synthesis of highly valuable functionalized 1,4-diketone derivatives in good yields and with an excellent diastereoselectivity. The established method provides a rapid approach to structurally diverse 1,4-diketone scaffold in a very mild and rapid fashion from simple starting materials. Moreover, the protocol could be easily scaled up to gram-scale synthesis. An attempt to develop an asymmetric version of the Rh(I)/guanidine system was also explored, resulting in a moderate enantioselectivity (71% ee).
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