Iodine/potassium iodide catalyst for the synthesis of trifluoromethylated quinazolines via intramolecular cyclization of 2,2,2-trifluoro-N-benzyl-N′-arylacetimidamides View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-03-13

AUTHORS

Ali Darehkordi, Elham Kazemi

ABSTRACT

An efficient and simple protocol for the synthesis of trifluoromethylated quinazolines has been described by I2-/KI-promoted oxidative C(sp3)-C(sp2) bond under the optimal oxidative cyclization reaction conditions. The required 2,2,2-trifluoro-N-benzyl-N'-arylacetimidamides are readily prepared from the corresponding acetimidoyl chlorides and benzylamines under a nucleophilic substitution reaction in the form of in situ. The merits of this protocol are the use of inexpensive molecular iodine, metal-free oxidative coupling and good to excellent yields. More... »

PAGES

1-9

References to SciGraph publications

  • 2016-08. Synthesis of novel fused quinazolinone derivatives in MOLECULAR DIVERSITY
  • Journal

    TITLE

    Molecular Diversity

    ISSUE

    N/A

    VOLUME

    N/A

    Author Affiliations

    Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s11030-019-09933-8

    DOI

    http://dx.doi.org/10.1007/s11030-019-09933-8

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1112731852

    PUBMED

    https://www.ncbi.nlm.nih.gov/pubmed/30868331


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