Regioselective synthesis of pyrimidine-fused tetrahydropyridines and pyridines by microwave-assisted one-pot reaction View Full Text


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Article Info

DATE

2019-03-07

AUTHORS

Pooja Kumari, Rahul Yadav, Ruchi Bharti, Tasneem Parvin

ABSTRACT

A regioselective three-component reaction of α,β-unsaturated aldehydes, cyclic 1,3-dicarbonyls and 6-aminouracils in the presence of FeCl3·6H2O as catalyst under microwave irradiation has been demonstrated. Three-component reaction of α,β-unsaturated aldehydes like cinnamaldehyde/crotonaldehyde, cyclic 1,3-diketones such as 2-hydroxy-1,4-naphthaquinone/dimedone and 6-aminouracils provides regioselective pyrimidine-fused tetrahydropyridines tethered with cyclic 1,3-diketones. On the other hand, replacing cyclic 1,3-diketones by 4-hydroxycoumarin and keeping all other conditions the same provided a two-component pyrimidine-fused pyridines. The salient features of this methodology are operational simplicity, short reaction time, good-to-moderate yields of the products, easy purification method and regioselective products having medicinally important heterocyclic rings such as pyrimidine, tetrahydropyridine or pyridine. More... »

PAGES

1-11

Journal

TITLE

Molecular Diversity

ISSUE

N/A

VOLUME

N/A

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11030-019-09929-4

DOI

http://dx.doi.org/10.1007/s11030-019-09929-4

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1112585934

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30843127


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