Heat transfer analysis during the hydrothermal degradation of an epoxy resin using differential scanning calorimetry (DSC) View Full Text


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Article Info

DATE

2016-08

AUTHORS

Gidéon Simenou, Eric Le Gal La Salle, Jean-Luc Bailleul, Jérôme Bellettre

ABSTRACT

In the present work, an epoxy-amine-cured resin is subjected to hydrothermal degradation, in high-temperature and high-pressure water. The thermal behaviour of the epoxy-amine-cured resin, during the hydrothermal degradation, was characterized, by differential scanning calorimetry using high-pressure and high-temperature crucibles. The study is performed by heating samples from ambient temperature to a bearing temperature between 335 and 390 °C. Operating pressure at these bearing temperatures can exceed 400 bar. The complete degradation of the resin can be achieved at 335 °C, but only for nonzero resident times (IE, maintaining the heating at the bearing temperature), regardless of the bearing temperature. At a specific temperature level, an exothermic heat flux is observed, when heating both water only (system 1) and water + resin (system 2). We have shown that this exothermic heat flux is due to a phase transition. More... »

PAGES

861-869

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10973-016-5443-5

DOI

http://dx.doi.org/10.1007/s10973-016-5443-5

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https://app.dimensions.ai/details/publication/pub.1025083923


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