The effect of melt flow index, melt flow rate, and particle size on the thermal degradation of commercial high density ... View Full Text


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Article Info

DATE

2013-12

AUTHORS

Mehrdad Seifali Abbas-Abadi, Mehdi Nekoomanesh Haghighi, Hamid Yeganeh, Babak Bozorgi

ABSTRACT

The powder of EX5 grade of high density polyethylene—without any additives—manufactured by Amirkabir petrochemical company was separated by shaker equipment. The separated powder of average diameter ~25, ~62.5, ~87.5, ~112.5, ~137.5, ~175 and the particles >200 μm was tested by a thermogravimetric (TG) analysis instrument in nitrogen atmosphere and heating rates of 10, 20, and 30 °C min−1. In addition, the separated powders were analyzed by a melt flow index (MFI) instrument, and the viscosity average molecular mass (Mv) of the powders was tested by a viscometer. Kinetic evaluations were performed by Friedman and Kissinger analysis methods and apparent activation energy for the overall degradation of the powders was determined. The effects of molecular mass, MFI, MFR, and particle size on the degradation TG curve, derivative thermogravimetry curve breadth, and activation energy of thermal degradation were considered. The results showed that the Mv of EX5 pipe grade produced by two serial reactors is increased by increasing of the particle size and, MFI is decreased with a little deviation by particle size increasing. The particle size has no obvious effect on the melt flow rate (MFR), and MFR as function of molecular mass distribution does not change very much. The results showed that the powder with bigger particles and higher molecular mass moderately increases the activation energy and shifts the degradation curve to the higher temperatures. More... »

PAGES

1333-1339

References to SciGraph publications

  • 2004-01. Three model-free methods for calculation of activation energy in TG in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2004-04. Isoconversional methods in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2011-02. Copyrolysis of block polypropylene with waste wood chip in KOREAN JOURNAL OF CHEMICAL ENGINEERING
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