Thermal and morphological study of Al2O3 nanofibers derived from boehmite precursor View Full Text


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Article Info

DATE

2011-10-13

AUTHORS

Lingli Peng, Xiangyu Xu, Zhi Lv, Jiaqing Song, Mingyuan He, Qian Wang, Lijun Yan, Yang Li, Zhaofei Li

ABSTRACT

The boehmite nanofibers were prepared by using NaAlO2 and Al2(SO4)3 as the starting materials without any surfactant. The phase transitions of the boehmite nanofibres against different temperature were studied and various phases were derived from well-crystallized boehmite nanofibers. All these phases had the same morphology even after high temperature calcination. In addition, the retention of specific surface area of the samples were very high because of the limited aggregation occurred in calcinations for each sample. For instance, the γ-Al2O3 obtained at 500 °C had the specific surface area (208.56 m2/g) with an average pore diameter of 6.0 nm. With the further increase of the calcination temperature, the nanofibers became shorter and coarsening, which resulted in the decrease of the specific surface area. It is worthwhile to notice that the BET surface areas (40.97 m2/g) and the pore volume (0.27 cm3/g) of the fibrous structures obtained after 1200 °C calcination are substantially higher than that of the non-fibrous alumina because of the morphology maintenance. More... »

PAGES

749-754

References to SciGraph publications

  • 2002-07. Morphological and structural change of nano-pored alumina membrane above 1200 K in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2002-03. Thermal decomposition of bauxite minerals: infrared emission spectroscopy of gibbsite, boehmite and diaspore in JOURNAL OF MATERIALS SCIENCE
  • 2009-07. Role of the dispersion route on the phase transformation of a nano-crystalline transition alumina in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2009-04-27. Sintering of a nano-crystalline metastable alumina in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2005-08. A comparative study of the effects of decomposition rate control and mechanical grinding on the thermal decomposition of aluminum hydroxide in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2007-07-11. XRD, TEM and thermal analysis of Fe doped boehmite nanofibres and nanosheets in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2009-06-19. Evaluation of thermal protective performance of basalt fiber nonwoven fabrics in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2009-08-07. Effect of zeolite, kaolin and alumina during cracking of heavy petroleum residue evaluated by thermogravimetry in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2008-08-12. XRD, TEM and thermal analysis of yttrium doped boehmite nanofibres and nanosheets in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2009-06-10. Thermal decomposition of Bayer precipitates formed at varying temperatures in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2003-03. Emanation thermal analysis study of synthetic gibbsite in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
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